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Tipo: Artigo de Evento
Título : Synthesis and caracterization of CTO (CaTiO3)
Autor : Silva, Marcelo Antonio Santos da
Fernandes, Tatiana Sainara Maia
Santiago, Alexander Arley Xavier
Sales, Juscelino Chaves
Sombra, Antônio Sérgio Bezerra
Palabras clave : Método de sinestesia no estado sólido;Difração de raios - X;Refinamento
Fecha de publicación : 2011
Citación : SILVA, Marcelo Antonio Santos da; FERNANDES, Tatiana Sainara Maia; SANTIAGO, Alexander Arley Xavier; SALES, Juscelino Chaves; SOMBRA, Antônio Sérgio Bezerra. Synthesis and caracterization of CTO (CaTiO3). In: CONGRESSO BRASILEIRO DE CERÂMICA, 55º, 29 maio a 01 jun. 2011, Porto de Galinhas, Pernambuco, Brasil. Anais[…] Porto de Galinhas, Pernambuco, 2011.
Abstract: The objective of this work is to study the ceramic material CTO (CaTiO3) by X-Ray Diffraction. The composites of CTO are widely used in dielectric resonators in communication systems. The CTO was prepared by solid state method in a planetary high energy ball milling (Fritsch Pulverisette 5). Stoichiometric quantities of CaCO3 (Aldrich 99%) and TiO2 (Merck 99%) were dry milled during 4h with a rotational speed of 370 rpm and then calcined at 1000 ºC for 3h. After, the CTO was studied by X-ray diffraction (XRD). The refinament showed that the CTO was formed with 100% mass, the graph of Williamson-Hall showed a homogeneous sample, with a contraction in the crystal lattice and a reasonably small particle size.
URI : http://www.repositorio.ufc.br/handle/riufc/55882
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